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ACQUITY UPLC CSH C18 Column
面议
ACQUITY UPLC CSH Phenyl-Hexyl Column
面议
ACQUITY UPLC HSS T3 Column
面议
ACQUITY UPLC HSS PFP Column
面议
ACQUITY UPLC BEH HILIC柱
面议
ACQUITY UPLC BEH Phenyl Column
面议
ACQUITY UPLC BEH Amide Column
面议
ACQUITY UPLC HSS Cyano Column
面议
ACQUITY UPLC HSS C18 （SB）Column
面议
ACQUITY UPLC系统
面议
Alliance HPLC系统
面议
Breeze QS HPLC系统
面议ACQUITY UPLC BEH Shield RP18柱，除了C18链以外还包括一个亲水的氨基甲酸酯官能团(极性内嵌)，从而对碱性分析物提供优异的峰形。该色谱柱也提供相对于直链烷基色谱柱的其它选择性。
1.7 µm的亚乙基桥杂化颗粒[BEH]是UPLC®技术得以实现的关键要素之一。该产品目前提供三种不同的粒径[130Å、200Å和300Å]以及几种用于反相色谱和亲水作用色谱的键合相，适用于从小分子分析到大分子生物制药分析的各类应用。杂化颗粒技术因其固有的化学稳定性而能采用更宽的pH范围[pH 1-12]，从而可为方法开发提供一种通用且可靠的分离技术。
UPLC法测定地黄叶及块根中的梓醇和毛蕊花糖苷
目的比较地黄叶及块根中梓醇和毛蕊花糖苷的含有量.方法地黄叶及块根甲醇提取液的分析采用ACQUITY UPLC BEH Shield RP18色谱柱(2.1 mm×100 mm,1.7μm);柱温35℃;流动相为乙腈-0.1%磷酸水溶液,梯度洗脱;体积流量0.2 m L/min;检测波长210 nm.结果梓醇含有量由高到低,依次为地黄嫩叶(149.22 mg/g)老叶(49.29 mg/g)块根(33.33 mg/g)干叶(15.53 mg/g);毛蕊花糖苷含有量依次为地黄老叶(10.27 mg/g)干叶(10.03 mg/g)嫩叶(9.56 mg/g)块根(0.28 mg/g).结论地黄嫩叶中梓醇的含有量约为老叶的3倍,但毛蕊花糖苷的含有量略低于老叶.地黄叶存放一年后,毛蕊花糖苷的减少量比梓醇小,表明前者稳定性高于后者.而且,这两种成分在叶中的含有量均比在块根中更高.
品名 | 编号 |
ACQUITY - XBridge BEH Shield RP18 Method Transfer Kit, 130Å, 1.7 - 3.5 µm, 2.1 - 4.6 mm X 50 - 100... | 186004965 |
ACQUITY - XBridge BEH Shield RP18 Method Transfer Kit, 130Å, 1.7 - 5 µm, 2.1 - 4.6 mm X 50 - 150mm... | 186004959 |
ACQUITY - XBridge BEH Shield RP18 Method Transfer Kit, 130Å, 1.7 - 3.5 µm, 2.1 - 4.6 mm X 100 - 15... | 186004972 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 1 mm X 100 mm, 3/pkg | 176000875 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 1 mm X 50 mm, 3/pkg | 176000874 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 1 mm X 150 mm, 1/pkg | 186003373 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 1 mm X 100 mm, 1/pkg | 186002852 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 1 mm X 50 mm, 1/pkg | 186002851 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 1 mm X 150 mm, 3/pkg | 176001045 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 50 mm, 3/pkg | 176000876 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 30 mm, 1/pkg | 186003909 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 150 mm, 1/pkg | 186003376 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 100 mm, 1/pkg | 186004669 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 100 mm, 1/pkg | 186002854 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 50 mm, 1/pkg | 186002853 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 100 mm, 3/pkg | 176000877 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 30 mm, 1/pkg | 186004667 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 50 mm, 1/pkg | 186004668 |
ACQUITY UPLC BEH Shield RP18 Method Validation Kit, 130Å, 1.7 µm, 2.1 mm X 150 mm, 3/pkg | 186006021 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 150 mm, 3/pkg | 176001049 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 150 mm, 3/pkg | 176001805 |
ACQUITY UPLC BEH Shield RP18 Method Validation Kit, 130Å, 1.7 µm, 2.1 mm X 50 mm, 3/pkg | 186004048 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 50 mm, 3/pkg | 176001803 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 100 mm, 3/pkg | 176001804 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 30 mm, 3/pkg | 176001802 |
ACQUITY UPLC BEH Shield RP18 VanGuard Pre-column, 130Å, 1.7 µm, 2.1 mm X 5 mm, 3/pkg | 186003977 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 2.1 mm X 30 mm, 3/pkg | 176001309 |
ACQUITY UPLC BEH Shield RP18 Method Validation Kit, 130Å, 1.7 µm, 3 mm X 100 mm, 3/pkg | 186004696 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 150 mm, 1/pkg | 186004670 |
ACQUITY UPLC BEH Shield RP18 Column, 130Å, 1.7 µm, 3 mm X 75 mm, 1/pkg | 186005610 |
ACQUITY UPLC BEH Shield RP18 Method Validation Kit, 130Å, 1.7 µm, 3 mm X 50 mm, 3/pkg | 186004695 |
ACQUITY UPLC BEH Shield RP18 Method Validation Kit, 130Å, 1.7 µm, 2.1 mm X 100 mm, 3/pkg | 186004049 |
